Instrumental Gas Analysis (IGA)

Instrumental gas analysis (IGA) measures gas-forming elements (C, H, O, N and S) present in solid materials from ppm to percentage levels. A high temperature furnace is used to rapidly heat the sample and thereby convert certain elements into volatile forms in order to separate and measure them.

Instrumental Gas Analysis (IGA) technique from Evans Analytical Group (EAG).Carbon and sulfur are measured based on combustion and infrared detection. The analytical method is based on the complete oxidation of the solid sample by combustion in an oxygen plasma (above 2000°C). The sample is placed in a ceramic crucible in a high frequency induction furnace where it is heated. The combustion of the sample releases various gases, which are measured by four infrared detectors. The analysis of SO2 determines the sulfur content. The analysis of CO and CO2 determines the carbon content.

Nitrogen, oxygen and hydrogen are measured using inert gas fusion or solid carrier gas heat extraction. The sample is placed in a graphite crucible and inserted into a furnace, where it is held between the electrodes. After purging with an inert gas (He or Ar), a high current is passed through the crucible, creating a temperature increase (above 2500 ºC). Any gases generated in the furnace (CO, CO2, N2 and H2) are released into a flowing inert gas stream, which is directed to the appropriate detector: infrared for O measured as CO, or thermal conductivity for N and H measured by TCD. Instrument calibration is performed using known reference materials.


For Trace Elemental Analysis using GDMS, IGA, ICP-OES or LA-ICP-MS:

Evans Analytical Group (New York) - Sample Submittal Form (English, pdf)
Evans Analytical Group SAS (France) - Sample Submittal Form (English, pdf)
Evans Analytical Group SAS (France) - Sample Submittal Form (French, pdf)

 

  • H, C, S, N and O determination in solids, powders or particulate materials
  • Fractional gas analysis to quantify C, H, O, N and S
  • For differentiating surface and bulk concentrations of H, O and N

Signal Detected: Infrared absorption and/or thermal conductivity

Elements Detected: H, C, N, O and S

Detection Limits: ppm

Depth Resolution: Bulk technique

  • Accurate determination of gas-forming elements from ppm to wt%
  • Can provide H and O environment information (surface or bulk) using temperature programs and reaction agents
  • Requires large amount of sample (10mg to g range)
  • Sputter targets
  • Semiconductor materials manufacturing
  • Steel industry
  • Metal alloys
  • Powder metallurgy
  • Chemicals (Catalysts)
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