Polymer Case Study: Cracking of Molded Components

Used for everything from electronics to basic personal care items, injection molded plastic components are an essential part of most of today’s consumer products. These parts help create durable, cost-effective goods to meet consumer demand.

Case Study

An injection molded component in a consumer product was found to have an increased failure rate over a three-month period. The part contained a polyolefin copolymer and an inorganic filler.

Analysis​

Comparisons were made between failed and control parts. Based on NMR spectroscopy, it was found that the failed sample had a different relative ratio of monomers compared to the control sample. 

In addition, based on EDS elemental analysis of ash from loss on ignition testing, the inorganic filler material was found to contain different elements.

Result​

These compositional differences were traced back to out-of-specification resins and issues with the raw material supply chain.

Failure Analysis of Polymers ​

For more than 50 years, scientists and engineers at Eurofins EAG have investigated and resolved product failures for clients. Our team of experts identify key failure indicators and follow them to the root cause.

Polymeric Materials Evaluated at EAG​

Failure analysis of plastics, thermosets, and rubber materials is commonly performed on finished products and typically involve comparative analysis between failed and non-failed samples. Once the potential root cause is identified, experiments can be designed and conducted to test the hypothesis and recreate the failure in the laboratory. Eurofins EAG can evaluate a variety of polymer types, including:

  • Raw materials in polymer formulations
  • Adhesives (heat/moisture/UV-cured, silicones, epoxies, acrylates)
  • Coatings (functional or decorative)
  • Thermoplastics, thermosets, thermoplastic elastomers, composites
  • Molded, extruded, cast components


Eurofins EAG Laboratories offers a full suite of analytical techniques to evaluate the identity, composition, morphology, topography, and rheology of polymeric materials and components.

  • Chromatography: GC, GC-MS, HPLC, IC, LC-MS, Pyrolysis GC-MS, HS/TD/SPME GC-MS
  • Inorganic Identification and Quantification: ICP-MS, ICP-OES, SEM-EDS, XRD, XRF
  • Physical Testing: Contact Angle, Mechanical Testing, Rheometry, Viscometry
  • Spectroscopy: Ellipsometry, FTIR, NIR, NMR, Raman, UV-Vis
  • Surface Analysis: Auger, SEM, TOF-SIMS, XPS
  • Surface Metrology: AFM, Nanoindentation, Profilometry
  • Thermal Analysis: DMA, DSC, RGA, TGA, TGA-IR, TGA-MS, TMA

Contact Our Team

Call +1 800-366-3867 or email us.

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